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透明沸石膜的製作方法及其結構 METHOD FOR MAKING TRANSPARENT CONTINUOUS ZEOLITE FILM AND STRUCTURE OF THE ZEOLITE FILM
專利名稱 METHOD FOR MAKING TRANSPARENT ZEOLITE FILM AND STRUCTURE OF THE ZEOLITE FILM
申請日 (校編號) 2004/09/15  (092025US)
2003/09/30  (092025TW)
專利證書號 7,253,130 美國
I240648 中華民國
專利權人 國立中央大學
發明人 蔣孝澈、許哲豪、劉家銘、羅希達


技術摘要:
A method for making transparent continuous zeolite film is provided. First a transparent precursor sol is prepared, and the precursor sol is processed to a specific concentration. The precursor solution is coated on a surface of a substrate which is heated under an ambiance of 120.about.250.degree. C. in temperature and a humidity less than saturated humidity. The packing of zeolite nanocrystals in the film converted from coated precursor sol has preferred orientation and the film shows super-hydrophobic property. 一種透明沸石膜的製作方法係先加熱包含矽源、金屬原子、水及沸石結構導引分子之混合溶液,以配製出濃縮的可產生沸石之溶液,其中加熱溫度低於攝氏100度,且加熱程序係在形成懸浮沸石前停止,再稀釋可產生沸石之溶液。之後,將可產生沸石之溶液塗佈在基材上,再在攝氏120到250度之溫度下以低於飽和溼度進行處理,以使塗佈於基材上的可產生沸石之溶液轉化為一沸石結晶膜,其中相對溼度係控制在30%到98%間。所獲得之沸石結晶膜有一定排列次序或有疏水性,且因為所形成沸石膜中之沸石結晶及結晶間孔隙皆為奈米尺度故呈現透明。

解決的問題或達成的功效:
The present invention provides a method to avoid the disadvantages associated with the above known prior arts for forming zeolite films and to present a new and easier procedure for the preparation of a continuous, transparent and preferred oriented film of zeolite on substrate. 提供一種透明沸石膜的製作方法,可以較簡單的步驟製備有次序排列之透明沸石膜。

應用領域:
The present invention relates to the preparation of a zeolite film on a substrate, and more particularly to the preparation of a continuous and transparent zeolite film having substantial preferred crystallographic orientation on a substrate. 此種膜係呈現透明狀而可應用於觸媒、光學、偵測器及電子產品,甚至可以作為保護膜、抗刮膜、阻絕膜或作為其他功能型鍍膜之基礎。

適用產品:


IPC:
B01J-020/18(2006.01); (IPC 1-7) : B01J-020/18

Claim 1:
1. A method for producing a transparent zeolite film, comprising: A. preparing a precursor sol capable of forming zeolite; B. processing the precursor sol to a specific concentration; C. coating the precursor sol to a surface of a substrate; and D. heating the coated substrate under a temperature between about 120.degree. C. and about 250.degree. C., and under a humidity less than a saturated humidity to convert the precursor sol to the transparent zeolite film. 1.一種透明沸石膜的製作方法,包括: (a)加熱一混合溶液,該混合溶液包含一矽源、一金屬原子、水及一沸石結構導引分子(SDA),以配製出濃縮的一可界生沸石之溶液,其中加熱該泥合溶液的溫度係低於攝氏100度,且加熱該混合溶液的程序係在形成懸浮沸石前停止; (b)稀釋該可產生沸石之溶液; (c)將該可產生沸石之溶液塗佈在一基材上;以及 (d)將塗佈後之該基材在攝氏120到250度之溫度下以低於一飽和溼度進行處理,以使塗佈於該基材上的該可產生沸石之溶液轉化為透明的一沸石結晶膜,其中相對溼度係控制在30%到98%間。

聯繫方式
聯絡人:研發處智權技轉組 與我連絡
電話:03-4227151 #27076、27077 網址:http://www.caic.ncu.edu.tw/
地 址: 32001桃園市中壢區中大路300號
 
                 
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